N-苯基-2-[2-(苯基氨基甲酰)苯基]二硒基苯甲酰胺合成路线 (共 19 条)
反应条件
1: 88 percent / acetonitrile / 3 h / Ambient temperature
2: 99 percent / N2H4*H2O / ethanol / Heating
View Scheme
参考文献
Mlochowski, Jacek; Kloc, Krystian; Syper, Ludwik; Inglot, Anna D.; Piasecki, Egbert
Liebigs Annalen der Chemie, 1993 , # 12 p. 1239 - 1244
反应条件
1: dimethylformamide / 1 h / 130 °C
2: methanol
3: 33percent aq. MeNH2 / methanol / 1 h
View Scheme
参考文献
Fisher, Hartmut; Dereu, Norbert
Bulletin des Societes Chimiques Belges, 1987 , vol. 96, # 10 p. 757 - 768
反应条件
dihydrogen peroxide in chloroform-d1
参考文献
Sarma, Bani Kanta; Mugesh, Govindasamy
Chemistry - A European Journal, 2008 , vol. 14, # 34 p. 10603 - 10614
反应条件
methylamine in methanol
1 h; Yield given;
参考文献
Fisher, Hartmut; Dereu, Norbert
Bulletin des Societes Chimiques Belges, 1987 , vol. 96, # 10 p. 757 - 768
反应条件
meta-chloroperoxybenzoic acid; 2,2'-azo-bisisobutyronitrile; triphenylstannane
1.) benzene, reflux; 2.) benzene, reflux; Yield given. Multistep reaction;
参考文献
Fong, Mei C.; Schiesser, Carl H.
Tetrahedron Letters, 1995 , vol. 36, # 40 p. 7329 - 7332
反应条件
sodium hydroxide in methanol
T=80°C; other alcohols as solvents; solvent isotope effect; var. time, temp. and pH; Rate constantEquilibrium constantMechanism;
参考文献
Kawai, Yukinori; Matsubayashi, Kyuichi
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 8 p. 1561 - 1566
反应条件
in dichloromethane
1 h; Mechanism;
参考文献
Fisher, Hartmut; Dereu, Norbert
Bulletin des Societes Chimiques Belges, 1987 , vol. 96, # 10 p. 757 - 768
反应条件
in chlorobenzene
T=120°C;
参考文献
Fong, Mei C.; Schiesser, Carl H.
Journal of Organic Chemistry, 1997 , vol. 62, # 10 p. 3103 - 3108
反应条件
di-tert-butyl peroxide
参考文献
Fong, Mei C.; Gable, Robert W.; Schiesser, Carl H.
Acta Crystallographica Section C: Crystal Structure Communications, 1996 , vol. 52, # 8 p. 1886 - 1889