Bellegarde, B.; Pereyre, M.; Valade, J.
Bulletin de la Societe Chimique de France, 1967 , p. 3082 - 3083
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Gmelin Handbook: Sn: Org.Verb.4, 1.2.2.1.5.1, page 104 - 105
in neat (no solvent) byproducts: CH3OH; org. compd. addn. (syringe) to Sn-compd. (stirring) (exothermic rection provokes reflux of formed methanol after some min), mixt. stirring for 2h, MeOH vac. removal;
heating Sn- and org. compds. mixt. at 70°C for 2 h; vac. fractionation; elem. anal.;
参考文献
Voronkov, M. G.; Mirskov, R. G.; Kuznetsova, G. V.; Yarosh, N. K.; Yarosh, O. G.; et al.
Journal of General Chemistry USSR (English Translation), 1982 , vol. 52, p. 1612 - 1616
Zhurnal Obshchei Khimii, 1982 , vol. 52, p. 1820 - 1824
heating Sn- and org. compds. mixt. at 70°C for 2 h; vac. fractionation; elem. anal.;
参考文献
Voronkov, M. G.; Mirskov, R. G.; Kuznetsova, G. V.; Yarosh, N. K.; Yarosh, O. G.; et al.
Journal of General Chemistry USSR (English Translation), 1982 , vol. 52, p. 1612 - 1616
Zhurnal Obshchei Khimii, 1982 , vol. 52, p. 1820 - 1824
heating Sn- and org. compds. mixt. at 70°C for 2 h; vac. fractionation; elem. anal.;
参考文献
Voronkov, M. G.; Mirskov, R. G.; Kuznetsova, G. V.; Yarosh, N. K.; Yarosh, O. G.; et al.
Journal of General Chemistry USSR (English Translation), 1982 , vol. 52, p. 1612 - 1616
Zhurnal Obshchei Khimii, 1982 , vol. 52, p. 1820 - 1824
heating Sn- and org. compds. mixt. at 70°C for 2 h; vac. fractionation; elem. anal.;
参考文献
Voronkov, M. G.; Mirskov, R. G.; Kuznetsova, G. V.; Yarosh, N. K.; Yarosh, O. G.; et al.
Journal of General Chemistry USSR (English Translation), 1982 , vol. 52, p. 1612 - 1616
Zhurnal Obshchei Khimii, 1982 , vol. 52, p. 1820 - 1824
in neat (no solvent)
byproducts: methanol; org. compd. addn. gradually to Sn-compd. in evac. ampoule at room temp., after bulk methanol liberation reaction mixt. heating slowly to 125°C, then allowing to cool in air; recryst. (toluene/heptane); elem. anal.;
参考文献
Shcherbakov, V. I.; Stolyarova, N. E.; Trukhina, T. V.; Razuvaev, G. A.
Journal of General Chemistry USSR (English Translation), 1984 , vol. 54, p. 1841 - 1843
Zhurnal Obshchei Khimii, 1984 , vol. 54, p. 2062 - 2064
