5-氰基-3-吡啶甲酸甲酯合成路线 （共 4 条）
反应条件
palladium diacetate; triphenylphosphine on polystyrene in tetrahydrofuran T=140 - 155°C; 0.0416667 h; microwave irradiation;
参考文献
Srivastava, Rajiv R.; Zych, Andrew J.; Jenkins, David M.; Wang, Hong-Jun; Chen, Zhen-Jia; Fairfax, David J.
Synthetic Communications, 2007 , vol. 37, # 3 p. 431 - 438
反应条件
potassium permanganate; potassium carbonate; dimethyl sulfate in water; N,N-dimethyl-formamide; acetone
反应条件
in DMF (N,N-dimethyl-formamide) 15 h; Heating / reflux;
参考文献
ELI LILLY AND COMPANY
Patent: WO2005/66126 A1, 2005 ;
Location in patent: Page/Page column 66 ;
WO 2005/066126 A1
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran T=-78°C; 1.05 h; 2: With sodium hydroxide; water in tetrahydrofuran
参考文献
ELI LILLY AND COMPANY
Patent: WO2005/66126 A1, 2005 ;
Location in patent: Page/Page column 66-67 ;
WO 2005/066126 A1
