1: 60 percent / tributyltin hydride, AIBN / toluene; methanol / 1 h / Heating 2: 73 percent / 6 M HCl / methanol / 0.5 h / Heating View Scheme

1: 60 percent / tributyltin hydride, AIBN / toluene; methanol / 1 h / Heating 2: 73 percent / 6 M HCl / methanol / 0.5 h / Heating View Scheme

1: 60 percent / tributyltin hydride, AIBN / toluene; methanol / 1 h / Heating 2: 73 percent / 6 M HCl / methanol / 0.5 h / Heating View Scheme

1: 60 percent / tributyltin hydride, AIBN / toluene; methanol / 1 h / Heating 2: 73 percent / 6 M HCl / methanol / 0.5 h / Heating View Scheme

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '113916', constants.ctx, '0')">N-bromosuccinmide</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1731042', constants.ctx, '0')">chloroform</a> <br />1&nbsp;h;&nbsp;&nbsp;Ambient temperature;&nbsp;<br /> &nbsp;

<b>Multi-step reaction with 3 steps<br /> </b>1: 57 percent / diethyl azodicarboxylate, PPh₃ / tetrahydrofuran / 0.25 h / Ambient temperature; reactions of cyclohex-2-enol with diacylamines under Mitsunobu reaction conditions, stereocontrolled preparation of cyclohexane amino alcohols<br />2: 99 percent / sodium borohydride / propan-2-ol; H₂O / 1 h / 0 deg C -&gt; room temperature<br />3: 87 percent / NBS / CHCl₃ / 1 h / Ambient temperature<br /> <br /> &nbsp;