Unno, Masafumi; Kawaguchi, Yasuaki; Kishimoto, Yukiko; Matsumoto, Hideyuki
Journal of the American Chemical Society, 2005 , vol. 127, # 7 p. 2256 - 2263
in diethyl ether
grignard reagent in Et2O adding to Sn hydride soln. in Et2O, resulting Bu3SnMgCl adding dropwise to orthoformate in Et2O, stirring for 3 h, hydrolyzing, org. phase sepg.; purified by distn. in vacuo; NMR, IR and mass spectra;
参考文献
Quintard, Jean-Paul; Elissondo, Bernard; Mouko-Mpegna, David
Journal of Organometallic Chemistry, 1983 , vol. 251, # 2 p. 175 - 188
Semenov, V. V.; Ladilina, E. Yu.; Chesnokova, T. A.; Elistratova, N. K.; Kurskii, Yu. A.; Makarenko, N. P.
Russian Chemical Bulletin, 1995 , vol. 44, # 5 p. 927 - 930
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 1995 , # 5 p. 954 - 957
in diethyl ether
under N2, 0.9 equiv of i-PrMgCl in Et2O was added slowly over 5 h to stirred soln. of 1 equiv of (Me3Si)2NBCl2 in Et2O at 0°C, warmed toroom temp., stirred overnight; filtered, solvent removed, distd., redistilled; elem. anal.;
参考文献
Li, Bei-Li; Goodman, Mary A.; Neilson, Robert H.
Inorganic Chemistry, 1984 , vol. 23, p. 1368 - 1371
in diethyl ether
under N2, 0.9 equiv of i-PrMgCl in Et2O was added slowly over 5 h to stirred soln. of 1 equiv of (Me3Si)2NBCl2 in Et2O at 0°C, warmed toroom temp., stirred overnight; filtered, solvent removed, distd., redistilled; elem. anal.;
参考文献
Li, Bei-Li; Goodman, Mary A.; Neilson, Robert H.
Inorganic Chemistry, 1984 , vol. 23, p. 1368 - 1371
