反应条件
in tetrahydrofuran; diethyl ether addn. of TsiH in dry THF to MeLi in ether, stirred, 20h, 20°C, then reflux, 30min, dropwise addn. of anhydrous HgCl2 to refluxing soln.,further reflux, 5h, solvent removed;
参考文献
Eaborn, Colin; Retta, Negussie; Smith, J. David
Journal of Organometallic Chemistry, 1980 , vol. 190, # 1 p. 101 - 106