2,3,4-三-O-乙酰基吡喃戊糖合成路线 (共 2 条)
反应条件
1.1: dichloromethane / 1 h / 0 °C / Inert atmosphere 1.2: 0.5 h / 0 °C / Inert atmosphere 2.1: boron trifluoride dimethyl etherate / dichloromethane / 20 °C / Inert atmosphere 3.1: methanol; sodium methylate / 0.5 h / 20 °C View Scheme
参考文献
Touisni, Nadia; Maresca, Alfonso; McDonald, Paul C.; Lou, Yuanmei; Scozzafava, Andrea; Dedhar, Shoukat; Winum, Jean-Yves; Supuran, Claudiu T.
Journal of Medicinal Chemistry, 2011 , vol. 54, # 24 p. 8271 - 8277
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane T=-20°C; 4 h;
参考文献
Mori, Masato; Ito, Yukishige; Ogawa, Tomoya
Carbohydrate Research, 1990 , vol. 195, # 2 p. 199 - 224