1H-吡唑并[3,4-b]喹啉-3-胺合成路线 （共 7 条）
反应条件
hydrazine hydrate in ethanol 3 h; Heating;
参考文献
Srivastava, Ambika; Singh, Mrityunjay K.; Singh
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 1 p. 292 - 296
反应条件
1: 86 percent / aq. ammonia; cerium(IV) ammonium nitrate / 0 °C 2: 92 percent / hydrazine hydrate / 0.25 h / Heating View Scheme
参考文献
Praveen Kumar Darsi; Shiva Kumar; Rama Devi; Naidu; Dubey
Indian Journal of Heterocyclic Chemistry, 2012 , vol. 21, # 3 p. 237 - 244
反应条件
1: NH2OH*HCl; aq. NaOH / ethanol / 2 h / pH 8 / Heating 2: 90 percent / Ac2O / 2 h / Heating 3: 75 percent / POCl3 / 1 h / Heating 4: 75 percent / N2H4*H2O / 5 h / Heating View Scheme
参考文献
El-Sayed, Ola A.; Aboul-Enein, Hassan Y.
Archiv der Pharmazie, 2001 , vol. 334, # 4 p. 117 - 120
反应条件
1: thionyl chloride / benzene / 3 h / |Reflux 2: NH2NH2•xH2O / methanol / 0.25 h / |Reflux View Scheme
参考文献
Praveen Kumar Darsi; Shiva Kumar; Rama Devi; Naidu; Dubey
Indian Journal of Heterocyclic Chemistry, 2012 , vol. 21, # 3 p. 237 - 244
反应条件
1: 75 percent / POCl3 / 1 h / Heating 2: 75 percent / N2H4*H2O / 5 h / Heating View Scheme
参考文献
El-Sayed, Ola A.; Aboul-Enein, Hassan Y.
Archiv der Pharmazie, 2001 , vol. 334, # 4 p. 117 - 120
反应条件
1: 90 percent / Ac2O / 2 h / Heating 2: 75 percent / POCl3 / 1 h / Heating 3: 75 percent / N2H4*H2O / 5 h / Heating View Scheme
参考文献
El-Sayed, Ola A.; Aboul-Enein, Hassan Y.
Archiv der Pharmazie, 2001 , vol. 334, # 4 p. 117 - 120
反应条件
1: 82 percent / POCl3 / 80 - 90 °C 2: 86 percent / aq. ammonia; cerium(IV) ammonium nitrate / 0 °C 3: 92 percent / hydrazine hydrate / 0.25 h / Heating View Scheme
参考文献
Srivastava, Ambika; Singh, Mrityunjay K.; Singh
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 1 p. 292 - 296
