1: 80 percent / H2 / 0.2percent Pd/C / ethanol / 24 h / 40 - 50 °C / 760 Torr 2: 85 percent / 80percent H2SO4, H3BO3 / 1.5 h / 80 - 100 °C View Scheme
参考文献
Es'kin, A. P.; Gornostaev, L. M.; Zeibert, G. F.; Bogdanchikov, G. A.; El'tsov, A. V.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 1.2 p. 162 - 167
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 1 p. 188 - 194
With hydrogen; palladium on activated charcoal in ethanol T=40 - 50°C; P=760 Torr; 24 h;
参考文献
Es'kin, A. P.; Gornostaev, L. M.; Zeibert, G. F.; Bogdanchikov, G. A.; El'tsov, A. V. Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 1.2 p. 162 - 167Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 1 p. 188 - 194
Multi-step reaction with 2 steps 1: KOH / dioxane2: 71 percent / dioxane / 0.5 h
参考文献
Gornostaev, L. M.; Zeibert, G. F. Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, # 6 p. 1192 - 1194Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 6 p. 1323 - 1326
