n-butyllithium
1.) hexane, tetramethylenediamine, room temperature, 7 d, 2.) ether, room temperature, 0.5 h; Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Carter, Martin J.; Fleming, Ian; Percival, Alan
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2415 - 2434
hydroxocobalamine hydrochloride; lithium perchlorate in N,N-dimethyl-formamide
Ambient temperatureIrradiationelectrolysis at constant potential -0.95 V (vs. SCE);
参考文献
Scheffold, Rolf; Orlinski, Ryszard
Journal of the American Chemical Society, 1983 , vol. 105, # 24 p. 7200 - 7202