1: 4-methyl-benzoic acid With copper; sodium iodide in water
P=760.051 Torr; 1 h; Green chemistry;
2: 3-chloroprop-1-ene in water
P=760.051 Torr; 5 h; RefluxGreen chemistry;
参考文献
Liang, Zheng Yong; Wang, Li Li; Liu, Hui; Huang, Jin Shuo
Journal of the Chilean Chemical Society, 2013 , vol. 58, # 1 p. 1558 - 1561
in THF-d8 (tetrahydrofuran-d8)
-100°C; identified by NMR;
参考文献
Bartholomew, Erika R.; Bertz, Steven H.; Cope, Stephen; Murphy, Michael; Ogle, Craig A.
Journal of the American Chemical Society, 2008 , vol. 130, # 34 p. 11244 - 11245
1: 2-picoline With n-butyllithium in tetrahydrofuran; toluene
T=0 - 5°C; Metallation; 0.5 h;
2: 3-chloroprop-1-ene in tetrahydrofuran; toluene
T=0 - 5°C; Alkylation; 0.5 h;
参考文献
Van Der Schaaf, Paul A.; Kolly, Roman; Kirner, Hans-Juerg; Rime, Francois; Muehlebach, Andreas; Hafner, Andreas
Journal of Organometallic Chemistry, 2000 , vol. 606, # 1 p. 65 - 74
