in dichloromethane W-compd. and isocyanide stirred for 20 min, addn. of phosphine, stirred overnight; volume reduced, chromy. on an alumina column with CH2Cl2-hexane, evapn. of solvent, addn. of methanol; elem. anal.;
参考文献
Detter, Lisa D.; Conner, Kay A.; Rothwell, Arlene P.; Walton, Richard A.
Inorganica Chimica Acta, 1988 , vol. 143, p. 109 - 118
bis(benzonitrile)palladium(II) dichloride in benzene 20 h; Heatingfurther subst.; use of deallylation as deprotection of phenolic hydroxyl groups; Product distribution;
参考文献
Bruce, J. Malcolm; Roshan-Ali, Yusuf
Journal of Chemical Research, Miniprint, 1981 , # 7 p. 2564 - 2572
Chinese Chemical Letters, , vol. 23, # 6 p. 631 - 634
→
反应条件
in dichloromethane W-compd. and isocyanide stirred for 30 min, addn. of phosphine, stirred overnight; volume reduced, chromy. on an alumina column with CH2Cl2-hexane, solvent stripped off, addn. of petroleum ether, cooled to 0°C, recrystn. (CH2Cl2-petroleum ether); elem. anal.;
参考文献
Detter, Lisa D.; Conner, Kay A.; Rothwell, Arlene P.; Walton, Richard A.
Inorganica Chimica Acta, 1988 , vol. 143, p. 109 - 118
Agaev, U. Kh.; Kyazimov, Sh. K.; Ponomareva, G. Z.; Rzaeva, A. S.; Alieva, F. M.
J. Appl. Chem. USSR (Engl. Transl.), 1989 , vol. 62, # 8 p. 1894 - 1896,1765 - 1767
