Del'nik, V. B.; Kagna, S. Sh.; Katsnel'son, M. G.; Rabinovich, A. S.; Skop, S. L.
J. Gen. Chem. USSR (Engl. Transl.), 1981 , vol. 51, # 8 p. 1890 - 1894,1623 - 1626
Del'nik, V. B.; Kagna, S. Sh.; Katsnel'son, M. G.; Rabinovich, A. S.; Skop, S. L.
J. Gen. Chem. USSR (Engl. Transl.), 1981 , vol. 51, # 8 p. 1890 - 1894,1623 - 1626
hydrogen; dicobalt octacarbonyl T=120°C; P=225018 Torr; 0.0833333 h; var. temp., time, solv., reagent's and products' ratios; hidroquinone inhibitor adding: after O2 adding in order to oxidize the Co-catalyst; Product distribution;
参考文献
Katsnel'son; Del'nik; Kagna; Leenson
Journal of applied chemistry of the USSR, 1984 , vol. 57, # 12 pt 2 p. 2514 - 2517
hydrogen in chloroform dry solvents; degassing soln. of Mo-compd. and acrylonitrile dissolved in CHCl3 under 600 Torr of H2 at -196°C, stirring at 50°C (5 days); removal of solvent under reduced pressure, product mixt. not sepn., detn. by (1)H-NMR spectra;