反应条件
1: dimethyl N-cyano-dithioimidocarbonate With sodium sulfide in N,N-dimethyl-formamide
T=70°C; 2 h;
2: chloroacetonitrile in N,N-dimethyl-formamide
T=70°C; 2 h;
3: With potassium carbonate in N,N-dimethyl-formamide
T=70°C; 1 h; Further stages.;
参考文献
Thomae, David; Perspicace, Enrico; Hesse, Stephanie; Kirsch, Gilbert; Seck, Pierre
Tetrahedron, 2008 , vol. 64, # 39 p. 9309 - 9314