Journal of Chemical Research, Miniprint, , # 9 p. 2601 - 2623
→
反应条件
in water Kinetics; 25°C, 3 h, pH 2, reaction monitored by UV-spectroscopy;; separation by addn of pentane, complex identified by UV-spectroscopy, organic product by g.c.-m.s.;
参考文献
Marmion, Mary E.; Takeuchi, Kenneth J.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1988 , p. 2385 - 2392
in benzene a soln. of CH2=CHCH2OH and trans-Mo(N2)2(dppe)2 in benzene was refluxedfor 3 h under N2; cis- and trans-Mo(CO)2(dppe)2 were formed in 60percent total yield, conversion of CH2=CHCH2OH was 90-95percent;
参考文献
Lin, Yingrui; Lu, Xiyan
Journal of Organometallic Chemistry, 1983 , vol. 251, # 3 p. 321 - 326