air; sodium acetate; Pd on porous glass in N,N-dimethyl acetamide T=120°C; 3 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
1: allyl alcohol With α-cyclohexylcyclohexanemethanamine in water T=20°C; Heck reaction; 0.25 h; 2: 2-iodo aniline With 4'-hydroxyacetophenone oxime palladacycle catalyst in water T=120°C; Heck reaction; 14 h; Further stages.;
参考文献
Alacid, Emilio; Najera, Carmen
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 17-18 p. 2572 - 2584