2,4,4-三甲基-1-戊烯合成路线 (共 303 条)
反应条件
1: Cr2O3-H2SO4
2: sulfuric acid
3: boron fluoride / beim Erhitzen des Reaktionsgemisches mit wss. Natriumacetat-Loesung
View Scheme
参考文献
Man et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 3228
反应条件
lithium aluminium tetrahydride; oxygen
multistep reaction: 1) 85 deg C, 101,3 kPa, 67 h; Product distribution;
参考文献
Bilas, W.; Hoebold, W.; Pritzkow, W.
Journal fuer Praktische Chemie (Leipzig), 1982 , vol. 324, # 1 p. 125 - 141
反应条件
carbon disulfide; aluminium trichloride
参考文献
Bruson; Eastes
Journal of the American Chemical Society, 1938 , vol. 60, p. 2502,2504
反应条件
1: concentrated sulfuric acid / 20 - 25 °C
2: sodium ethylate; ethanol
View Scheme
参考文献
Goodrich Co.
Patent: US2460567 , 1944 ;
反应条件
1: Cr2O3-H2SO4
2: NaOBr
3: SOCl2
4: bromine
View Scheme
参考文献
Homeyer; Whitmore; Wallingford
Journal of the American Chemical Society, 1933 , vol. 55, p. 4209,4212
反应条件
sodium tetrahydroborate; Fe pythalocyanine; dimethylsulfide; oxygen in ethanol
T=20°C; P=760.051 Torr; 14 h;
参考文献
Hashimoto, Takuma; Hirose, Daisuke; Taniguchi, Tsuyoshi
Angewandte Chemie - International Edition, 2014 , vol. 53, # 10 p. 2730 - 2734
Angew. Chem., 2014 , vol. 126, # 10 p. 2768 - 2772,5
反应条件
aluminium trichloride; ammonia
1.) 35 deg C, 45 min; Yield given. Multistep reaction;
参考文献
Erre, Claude H.; Rousell, Christian
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 11-12 p. 449 - 453
反应条件
ammonium hydroxide; zinc(II) chloride
Yield given. Multistep reaction;
参考文献
Yurkovskaya, M. A.; Afanas'ev, A. Z.; Chertkov, V. A.; Bundel', Yu. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1988 , vol. 24, # 9 p. 1000 - 1008
Khimiya Geterotsiklicheskikh Soedinenii, 1988 , # 9 p. 1213 - 1221
反应条件
aluminium trichloride; ammonia
1.) 35 deg C, 45 min; Yield given. Multistep reaction;
参考文献
Erre, Claude H.; Rousell, Christian
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 11-12 p. 449 - 453
反应条件
dihydrogen peroxide; WO3; acetic acid
参考文献
Byers; Hickinbottom
Journal of the Chemical Society, 1948 , p. 1328,1329