2,4,4-三甲基-1-戊烯合成路线 (共 303 条)
反应条件
hydrogen iodide
T=0°C; man setzt das erhaltene Jodid bei 0grad mit Ag2O um;
参考文献
Komai, Takeshi; Matsuyama, Kazuo; Matsushima, Masaru
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, # 5 p. 1641 - 1646
反应条件
sulfuric acid
T=0 - 5°C;
参考文献
Ritter
Journal of the American Chemical Society, 1948 , vol. 70, p. 4253
反应条件
sodium hydroxide; sodium tetrahydroborate; boron trifluoride diethyl etherate; dihydrogen peroxide
1.) diglyme, 25-35 deg C, 1 h; 2.) diglyme, 25-35 deg C; Yield given. Multistep reaction;
参考文献
Brown, Herbert C.; Snyder, Carl; Rao, B. C. Subba; Zweifel, George
Tetrahedron, 1986 , vol. 42, # 20 p. 5505 - 5510
反应条件
lithium aluminium tetrahydride; oxygen
multistep reaction: 1) 85 deg C, 101,3 kPa, 67 h; Product distribution;
参考文献
Bilas, W.; Hoebold, W.; Pritzkow, W.
Journal fuer Praktische Chemie (Leipzig), 1982 , vol. 324, # 1 p. 125 - 141
反应条件
1: H2SO4 / acetic acid
2: H2SO4 / CHCl3
View Scheme
参考文献
Pospisil,J.; Taimr,L.
Collection of Czechoslovak Chemical Communications, 1964 , vol. 29, p. 381 - 389
反应条件
sulfuric acid in chloroform
参考文献
Pospisil,J.; Taimr,L.
Collection of Czechoslovak Chemical Communications, 1964 , vol. 29, p. 381 - 389
反应条件
1: KCl / liquid sulphur dioxide
2: water / und anschliessenden Erhitzen
View Scheme
参考文献
Graf,R.
Justus Liebigs Annalen der Chemie, 1963 , vol. 661, p. 111 - 157
参考文献
SUMITOMO CHEMICAL COMPANY, LIMITED
Patent: EP99752 B2, 1991 ;
反应条件
1: Cr2O3-H2SO4
2: NaOBr
3: SOCl2
4: water; NH3 / <10
View Scheme
参考文献
Homeyer; Whitmore; Wallingford
Journal of the American Chemical Society, 1933 , vol. 55, p. 4209,4212
反应条件
potassium hydroxide; polyethylene oxide in dichloromethane
参考文献
Goaller, R. Le; Slaoui, S.; Pierre, J. L.; Luche, J. L.
Synthetic Communications, 1982 , vol. 12, # 14 p. 1163 - 1169