2,4,4-三甲基-1-戊烯合成路线 (共 303 条)
反应条件
1: concentrated sulfuric acid / 20 - 25 °C
2: aqueous NaOH
View Scheme
参考文献
Niederl
Industrial and Engineering Chemistry, 1938 , vol. 30, p. 1269,1272
反应条件
benzene
T=190°C; Erwaermen des Reaktionsprodukts mit wss. Natriumcarbonat-Loesung;
参考文献
Alder; Soell
Justus Liebigs Annalen der Chemie, 1949 , vol. 565, p. 66
反应条件
Behandeln den erhaltenen Anhydrid mit Sodaloesung;
参考文献
Alder; Soell
Justus Liebigs Annalen der Chemie, 1949 , vol. 565, p. 66
反应条件
1: concentrated sulfuric acid / 20 - 25 °C
2: bromine / 85 °C
View Scheme
参考文献
Niederl
Industrial and Engineering Chemistry, 1938 , vol. 30, p. 1269,1272
反应条件
sulfuric acid
T=65°C;
参考文献
Ipatieff; Pines; Friedman
Journal of the American Chemical Society, 1938 , vol. 60, p. 2495
反应条件
1-butyl-3-methylimidazolium heptachlorodiindate (III)
T=80°C; 2 h; In ionic liquid; Product distribution / selectivity;
参考文献
SCHENECTADY INTERNATIONAL, INC.
Patent: WO2006/74401 A1, 2006 ;
Location in patent: Page/Page column 16-17 ;
反应条件
aluminium phenoxide
T=120 - 125°C; 20 h;
参考文献
Kahovec,J.; Pospisil,J.
Collection of Czechoslovak Chemical Communications, 1968 , vol. 33, p. 1709 - 1729
反应条件
sulfuric acid
T=25 - 30°C;
参考文献
Roehm and Haas Co.
Patent: US2106716 , 1936 ;
反应条件
1: 65percent H2O2 / H2O / 0 - 5 °C
2: 50percent H2O2 / H2O
View Scheme
参考文献
Komai, Takeshi; Matsuyama, Kazuo; Matsushima, Masaru
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, # 5 p. 1641 - 1646
反应条件
diethyl ether; dinitrogen tetraoxide
T=-5°C;
参考文献
Levy; Scaife
Journal of the Chemical Society, 1946 , p. 1094
Full Text Show Details
Baldock; Levy; Scaife
Journal of the Chemical Society, 1949 , p. 2627,2630