2-氯-N,N-二甲基乙胺合成路线 (共 199 条)
参考文献
Bayer and Co.
Patent: DE398010 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 1420
反应条件
ethanol; sodium ethanolate
参考文献
Zhurnal Obshchei Khimii, , vol. 29, p. 1012,1015; engl. Ausg. S. 992, 994
反应条件
anschliessendes Behandeln mit CH3I;
参考文献
Morren et al.
Journal de Pharmacie de Belgique, <NS> 7 <1952> 295, 302, 306
参考文献
Grail et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 1313
参考文献
Sperber et al.
Journal of the American Chemical Society, 1949 , vol. 71, p. 887,889
Full Text Show Details
Tilford et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 4001,4005
反应条件
anschliessend Behandeln mit CH3I;
参考文献
Morren et al.
Journal de Pharmacie de Belgique, <NS> 7 <1952> 295, 302, 306
反应条件
anschliessend Behandeln mit CH3I;
参考文献
J. Pharm. Belg. <NS>, , vol. 7, p. 295,302, 306
反应条件
sodium hydroxide in ethanol
参考文献
Murphy, Peter M; Phillips, Victoria A; Jennings, Sharon A; Garbett, Nichola C; Chaires, Jonathan B; Jenkins, Terence C; Wheelhouse, Richard T
Chemical communications (Cambridge, England), 2003 , # 10 p. 1160 - 1161
反应条件
1: Phenylborneol With Sodium hydride in toluene 1 h; Heating / reflux; 2: 2-chloro-N,N-dimethylaminoethane in toluene 4 h; Heating / reflux;
参考文献
Orion Corporation
Patent: US6335469 B1, 2002 ;
Location in patent: Example 2 ;
反应条件
1: Phenylborneol With sodium amide in 1,4-dioxane 2.5 h; Heating / reflux; 2: 2-chloro-N,N-dimethylaminoethane 4 h; Heating / reflux;
参考文献
Orion Corporation
Patent: US6335469 B1, 2002 ;
Location in patent: Example 1 ;