2-氯-N,N-二甲基乙胺合成路线 (共 199 条)
反应条件
Produkt5: 1,2-Bis-dimethylamino-aethan;
参考文献
Hromatka et al.
Monatshefte fuer Chemie, 1953 , vol. 84, p. 349,360
反应条件
sodium hydride in benzene 1. room temperature, 90 min; 2. 60 deg C, 30 min;
参考文献
Vejdelek; Metys; Holubek; et al.
Collection of Czechoslovak Chemical Communications, 1984 , vol. 49, # 11 p. 2649 - 2660
反应条件
sodium amide in toluene 4 h; Heating; Yield given;
参考文献
Cahiez, Gerard; Rivas-Enterrios, Jose; Clery, Patrick
Tetrahedron Letters, 1988 , vol. 29, # 30 p. 3659 - 3662
参考文献
Asta-Werke
Patent: DE952715 , 1952 ;
Full Text Show Details
Novak; Protiva
Collection of Czechoslovak Chemical Communications, 1959 , vol. 24, p. 3966,3974
反应条件
n-butyllithium 1.) THF, r.t., 2.) reflux; Yield given. Multistep reaction;
参考文献
Werner, Helmut; Hampp, Andreas; Peters, Karl; Peters, Eva Maria; Walz, Leonhard; Schnering, Hans Georg von
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1990 , vol. 45, # 11 p. 1548 - 1558
反应条件
potassium hydroxide in dimethyl sulfoxide 6 h;
参考文献
Shanazarov, A. K.; Granik, V. G.; Andreeva, N. I.; Golovina, S. M.; Mashkovskii, M. D.
Pharmaceutical Chemistry Journal, 1989 , vol. 23, # 10 p. 807 - 811
Khimiko-Farmatsevticheskii Zhurnal, 1989 , vol. 23, # 10 p. 1197 - 1200
反应条件
ethanol; sodium ethanolate
参考文献
Vejdalek et al.
Collection of Czechoslovak Chemical Communications, 1954 , vol. 19, p. 1274,1280
Chem.Abstr., 1955 , p. 336
反应条件
sodium amide; benzene
参考文献
Schmitt et al.
Annales Pharmaceutiques Francaises, 1956 , vol. 14, p. 566,578
反应条件
sodium hydrogencarbonate in acetone 6 h; Heating;
参考文献
McConnaughie; Jenkins
Journal of Medicinal Chemistry, 1995 , vol. 38, # 18 p. 3488 - 3501
参考文献
Cheney et al.
Journal of the American Chemical Society, 1949 , vol. 71, p. 60,62