N-重氮基氨基甲酸叔-丁基酯合成路线 （共 237 条）
反应条件
triethylamine in dimethyl sulfoxide
参考文献
Bulletin de la Societe Chimique de France, , p. 2543 - 2546
反应条件
triethylamine in 1,4-dioxane; water T=25°C;
参考文献
Rich, Daniel H.; Moon, Byung Jo; Boparai, Amrit S.
Journal of Organic Chemistry, 1980 , vol. 45, # 12 p. 2288 - 2290
反应条件
in diethyl ether 0.333333 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 58, # 18 p. 4791 - 4793
反应条件
in benzene T=80°C; 3 h;
参考文献
Journal of Organometallic Chemistry, , vol. 373, p. 133 - 142
反应条件
in benzene under nitrogen, proportions 7/1, refluxing for 3h at 80°C; removal of the solvent under reduced pressure, residue was chromd., elution with hexane/benzene(1/1), elution with dichloromethane/ethyl acetate;
参考文献
Journal of Organometallic Chemistry, , vol. 373, p. 133 - 142
反应条件
sodium hydroxide in 1,4-dioxane
参考文献
Pospisek,J.; Blaha,K.
Collection of Czechoslovak Chemical Communications, 1977 , vol. 42, p. 1069 - 1076
反应条件
potassium hydrogencarbonate in 1,4-dioxane; water
参考文献
Andruszkiewicz,R. et al.
Polish Journal of Chemistry, 1978 , vol. 52, p. 1167 - 1172
反应条件
in diethyl ether; dimethyl sulfoxide 1 h; Ambient temperature;
参考文献
Hansen, J. B.; Nielsen, M. C.; Ehrbar, U.; Buchardt, O.
Synthesis, 1982 , # 5 p. 404 - 405
反应条件
1: 73 percent / triethylamine / H2O; dioxane / 25 °C 2: 60 percent / diethyl ether / 1 h / 25 °C 3: 100 percent / sodium hydroxide, water / dioxane / pH 10 View Scheme
参考文献
Rich, Daniel H.; Moon, Byung Jo; Boparai, Amrit S.
Journal of Organic Chemistry, 1980 , vol. 45, # 12 p. 2288 - 2290
反应条件
triethylamine in N,N-dimethyl-formamide T=20 - 40°C;
参考文献
Liu, Jiawang; Wu, Guofeng; Cui, Guohui; Wang, Wei-Xuan; Zhao, Ming; Wang, Chao; Zhang, Ziding; Peng, Shiqi
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 17 p. 5672 - 5693
