N-重氮基氨基甲酸叔-丁基酯合成路线 （共 237 条）
反应条件
1: KHCO3 / H2O; dioxane 2: (i) EtOH, (ii) /BRN= 1363586/, dioxane 3: B2H6 View Scheme
参考文献
Polish Journal of Chemistry, , vol. 52, p. 1167 - 1172
反应条件
1: Et3N / dioxane; H2O 2: CrO3, Py / CH2Cl2 View Scheme
参考文献
Gray,C.J.; Parker,R.C.
Tetrahedron, 1975 , vol. 31, p. 2940 - 2943
反应条件
sodium carbonate in 1-dioxane-water; water
参考文献
Mead Johnson and Company
Patent: US4495194 A1, 1985 ;
反应条件
triethylamine in 1,4-dioxane; water T=50°C; 15 h;
参考文献
Jordis; Sauter; Siddiqi; Kuenburg; Bhattacharya
Synthesis, 1990 , vol. 1, # 10 p. 925 - 930
反应条件
(i) aq. NaOH, dioxane, (ii) /BRN= 102415/, Et2O; Multistep reaction;
参考文献
Keller-Schierlein; Widmer
Helvetica chimica acta, 1976 , vol. 59, # 6 p. 2021 - 2031
反应条件
in 1,4-dioxane; water 48 h; Ambient temperaturepH=10;
参考文献
Seprodi; Teplan; Magocsi; Medzihradszky
Acta Chimica Academiae Scientiarum Hungaricae, 1980 , vol. 104, # 3 p. 227 - 233
反应条件
1: triethylamine 3: water, sodium hydroxide View Scheme
参考文献
Rich, Daniel H.; Moon, Byung Jo; Boparai, Amrit S.
Journal of Organic Chemistry, 1980 , vol. 45, # 12 p. 2288 - 2290
反应条件
1: diethyl ether; dimethylsulfoxide / 1 h / Ambient temperature 2: HCl aq. / diethyl ether; H2O View Scheme
参考文献
Hansen, J. B.; Nielsen, M. C.; Ehrbar, U.; Buchardt, O.
Synthesis, 1982 , # 5 p. 404 - 405
反应条件
triethylamine in dimethyl sulfoxide
参考文献
Hansen, John B.; Buchardt, Ole
Journal of the Chemical Society, Chemical Communications, 1983 , # 4 p. 162 - 164
反应条件
1: 69.6 percent / Et3N / dioxane; H2O / 15 h / 50 °C 2: 81 percent / LiAlH4 / tetrahydrofuran / 1.) 0 deg C, 1 h, 2.) room temperature, 15 h 3: pyridine / 1.) 0 deg C, 2.) stored in the refrigerator for 5 days 4: 63.5 percent / 1.) Na/NH3 (liq.) / 1.) THF, temperature of liquid NH3, 2.) room temperature, 18.5 h View Scheme
参考文献
Baker, Gregory L.; Fritschel, Scott J.; Stille, John R.; Stille, John K.
Journal of Organic Chemistry, 1981 , vol. 46, # 14 p. 2954 - 2960
