N-重氮基氨基甲酸叔-丁基酯合成路线 (共 237 条)
参考文献
Justus Liebigs Annalen der Chemie, , vol. 702, p. 188 - 196
反应条件
1: 97 percent / dioxane; H2O / 48 h / 23 °C / pH 9.8 2: 81 percent / iodine / aq. acetic acid / 1 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 522 - 528
反应条件
sodium hydroxide; magnesium oxide in 1,4-dioxane
参考文献
Jorgensen,E.C. et al.
Journal of Medicinal Chemistry, 1971 , vol. 14, p. 899 - 903
反应条件
triethylamine in water; N,N-dimethyl-formamide T=40°C; 24 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 29, # 6 p. 1644 - 1654
反应条件
triethylamine in 1,4-dioxane 8 h;
参考文献
Pandey, Ganesh; Chakrabarti, Debasish
Tetrahedron Letters, 1996 , vol. 37, # 13 p. 2285 - 2288
反应条件
in 1,4-dioxane; sodium hydroxide; water T=20°C; 24 h;
参考文献
Dutt, Anita; Dutta, Arpita; Mondal, Raju; Spencer, Elinor C.; Howard, Judith A.K.; Pramanik, Animesh
Tetrahedron, 2007 , vol. 63, # 41 p. 10282 - 10289
反应条件
triethylamine in 1,4-dioxane; water
参考文献
Van Nispen; Bijl; Hendrix; Greven
Recueil des Travaux Chimiques des Pays Bas, 1983 , vol. 102, # 5 p. 276 - 283
反应条件
triethylamine in N,N-dimethyl-formamide T=20°C; pH=10; 48 h;
参考文献
Liu, Jiawang; Cui, Guohui; Zhao, Ming; Cui, Chunying; Ju, Jingfang; Peng, Shiqi
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 24 p. 7773 - 7788
反应条件
1: 92 percent / diethyl ether 2: 75 percent / toluene / 17 h / Heating 3: LiMCPBA / CH2Cl2 / 2 h / -78 °C 4: 35 percent / LiHMDS / tetrahydrofuran / -78 °C / 1.) 30 min, 2.) 30 min View Scheme
参考文献
Vidal, Joelle; Guy, Laure; Sterin, Sebastien; Collet, Andre
Journal of Organic Chemistry, 1993 , vol. 58, # 18 p. 4791 - 4793
反应条件
triethylamine in 1,4-dioxane; methanol; water 3 h; Ambient temperature;
参考文献
Nakamura, Takako; Matsuyama, Haruo; Kamigata, Nobumasa; Iyoda, Masahiko
Journal of Organic Chemistry, 1992 , vol. 57, # 14 p. 3783 - 3789