N-重氮基氨基甲酸叔-丁基酯合成路线 (共 237 条)
反应条件
(i) aq. K2CO3, (ii) /BRN= 1363586/, Py, (iii) aq. NaOH; Multistep reaction;
参考文献
Wuensch,E. et al.
Chemische Berichte, 1964 , vol. 97, p. 3298 - 3304
反应条件
sodium hydrogencarbonate
参考文献
Kato; Izumiya
Bulletin of the Chemical Society of Japan, 1966 , vol. 39, # 10 p. 2242 - 2249
反应条件
1: aq. Na2CO3 2: DCC View Scheme
参考文献
Hofmann,K. et al.
Journal of the American Chemical Society, 1965 , vol. 87, p. 611 - 619
反应条件
magnesium oxide in 1,4-dioxane; water
参考文献
Arold,H. et al.
Journal fuer Praktische Chemie (Leipzig), 1969 , vol. 311, p. 490 - 496
反应条件
1: 92 percent / diethyl ether 2: 75 percent / toluene / 17 h / Heating 3: LiMCPBA / CH2Cl2 / 2 h / -78 °C View Scheme
参考文献
Vidal, Joelle; Guy, Laure; Sterin, Sebastien; Collet, Andre
Journal of Organic Chemistry, 1993 , vol. 58, # 18 p. 4791 - 4793
反应条件
sodium hydrogencarbonate in 1,4-dioxane
参考文献
Kato; Izumiya
Bulletin of the Chemical Society of Japan, 1966 , vol. 39, # 10 p. 2242 - 2249
反应条件
sodium hydroxide in 1,4-dioxane
参考文献
Hofmann,K. et al.
Journal of the American Chemical Society, 1965 , vol. 87, p. 620 - 631
反应条件
1: dioxane 2: 90 percent / TMEDA; s-BuLi / -78 °C View Scheme
参考文献
Pandey, Ganesh; Reddy, Gottimukkula Devi; Chakrabarti, Debasish
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 2 p. 219 - 224
反应条件
triethylamine in 1,4-dioxane
5 h; Ambient temperature;
参考文献
Bodor, Nicholas; Sloan, Kenneth B.; Kaminski, James J.; Shih, Chung; Pogany, Stefano
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5280 - 5284
参考文献
Arold,H.; Reissmann,S.
Zeitschrift fuer Chemie (Stuttgart, Germany), 1968 , vol. 8, p. 107