1,1,1,3-四氯丙烷合成路线 (共 77 条)
反应条件
anhydrous iron chloride; diethylphosphoric acid ethyl ester; iron T=110 - 134°C; P=1875.19 - 6000.6 Torr; AutoclaveInert atmosphere;
参考文献
DAIKIN INDUSTRIES, LTD.; NOSE, Masatoshi; SUZUKI, Atsushi
Patent: WO2011/65574 A1, 2011 ;
Location in patent: Page/Page column 9-10 ;
反应条件
anhydrous diethylamine hydrochloride; 1,2-diphenyl-2-hydroxyethanone; iron(III) chloride in isopropyl alcohol Further byproducts given;
参考文献
Journal of Organic Chemistry, , vol. 37, p. 2633 - 2635
反应条件
1,2-diphenyl-2-hydroxyethanone; diethylamine; iron(III) chloride in isopropyl alcohol Further byproducts given;
参考文献
Journal of Organic Chemistry, , vol. 37, p. 2633 - 2635
反应条件
benzene; dibenzoyl peroxide T=70°C; P=20594.2 Torr;
反应条件
beim Chlorieren; zunaechst im Sonnenlicht in der Dampfphase, dann in fluessiger Phase unter Kuehlung;
参考文献
Journal of the American Chemical Society, , vol. 64, p. 1157
反应条件
anhydrous diethylamine hydrochloride; 1,2-diphenyl-2-hydroxyethanone in isopropyl alcohol Further byproducts given;
参考文献
Journal of Organic Chemistry, , vol. 37, p. 2633 - 2635
反应条件
anhydrous diethylamine hydrochloride; 1,2-diphenyl-2-hydroxyethanone; iron(III) chloride Further byproducts given;
参考文献
Journal of Organic Chemistry, , vol. 37, p. 2633 - 2635
反应条件
T=95°C; P=73550.8 Torr;
参考文献
Journal of the American Chemical Society, , vol. 70, p. 2531
Journal of the American Chemical Society, , vol. 69, p. 1104
US2440800 , ;
反应条件
FeIIFe2IIICl8(CH3CN)6 in N,N-dimethyl acetamide; acetonitrile T=130°C; P=15200 Torr; 4 h; other concentrations of CH3CN, DMA; other catalyst; Product distributionMechanism;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 39, # 12 p. 2534 - 2537
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , vol. 39, # 12 p. 2794 - 2798
反应条件
tetrachloromethane byproducts: C4H10, C2H6, C2H4; Irradiation (UV/VIS); for 120 h; further byproduct: CHCl3;
参考文献
Doklady Akademii Nauk SSSR, , vol. 132, p. 364 - 366
C.A., , p. 20973
Zhurnal Obshchei Khimii, , vol. 32, p. 2154 - 2160
Sn: Org.Verb.1, 1.1.1.2.4.7, page 73 - 76