1,1,1,3-四氯丙烷合成路线 （共 77 条）
参考文献
Haszeldine
Journal of the Chemical Society, 1953 , p. 3371,3377
反应条件
1: With potassium hydroxide; Aliquatreg; 336 in water
T=80°C; 3 h;
2: With chlorine
T=0°C; 3 h; UV-irradiation;
参考文献
TOKUYAMA CORPORATION; Hosaka, Shunsuke; Komatsu, Yasutaka; Moriwaki, Masayuki; Yamamoto, Kikuo; Okada, Naoya
Patent: US2013/165705 A1, 2013 ;
Location in patent: Paragraph 0156; 0157; 0158 ;
反应条件
anhydrous iron chloride; chlorine
T=82°C; P=1277.21 Torr; 15.33 h; Product distribution / selectivity;
参考文献
OCCIDENTAL CHEMICAL CORPORATION
Patent: WO2009/85862 A1, 2009 ;
Location in patent: Page/Page column 28 ;
反应条件
chlorine
T=100°C; Irradiation.mit UV-Licht;
参考文献
Ponomarenko; Snegowa
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 2067,2070; engl. Ausg. S. 2122, 2125
Full Text Show Details
Davis; Whaley
Journal of the American Chemical Society, 1951 , vol. 73, p. 2361
反应条件
T=185°C; mit UV-Licht.Irradiation;
参考文献
Ponomarenko; Snegowa
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 2067,2070; engl. Ausg. S. 2122, 2125
反应条件
pentacarbonyliron(0); N,N-dichloro-4-chlorobenzenesulfonamide in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=105°C;
参考文献
Rybakova,N.A. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1979 , vol. 28, p. 2433 - 2435
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1979 , vol. 28, # 11 p. 2618 - 2620
反应条件
trans-Mo(N2)2(1,2-bis(diphenylphosphino)ethane)2 in acetonitrile
T=140°C; 3 h; further reagents Mo(CO)6, Mo(CO)5PPh3, cis-Mo(CO)4(PPh3)2, cis-Mo(CO)4(dppe), cis-Mo(CO)2(dppe)2, MoH4(dppe)2;
参考文献
Zhiryukhina, N. P.; Chukovskaya, E. Ts.; Makhaev, V. D.; Borisov, A. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 3 p. 539 - 542
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 3 p. 600 - 603
反应条件
pentacarbonyliron(0)
T=120°C; 3 h; reaction of 1,1,1,3-tetrachloropropane with 1-hexene initiated by Fe(CO)5, Mo(CO)5 and Mn2(CO)10, conversion, effect of the nature of metal carbonyls, solvents; Product distribution;
参考文献
Chukovskaya, E. Ts.; Kuz'mina, N. A.; Rozhkova, M. A.; Freidlina, R. Kh.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 6 p. 1198 - 1202
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 6 p. 1345 - 1349
反应条件
bromine trifluoride; tin(IV) chloride in 1,2,2-trifluoro-trichloroethane
T=20 - 25°C;
参考文献
Kartashov, A. V.; Chuvatkin, N. N.; Boguslavskaya, L. S.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 12 p. 2276 - 2278
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 12 p. 2522 - 2525
反应条件
antimony(V) pentachloride; SbF3
Heating;
参考文献
Kost,V.N. et al.
Doklady Chemistry, 1960 , vol. 132, p. 569 - 571
Doklady Akademii Nauk SSSR, 1960 , vol. 132, p. 606 - 608
