3,3-二甲基-1-丁酸合成路线 (共 132 条)
反应条件
sulfuric acid T=5°C; 0.5 h;
参考文献
Randriamahefa, S.; Deschamps, P.; Gallo, R.; Grangette, H.
Synthesis, 1985 , # 5 p. 493 - 495
反应条件
1: Cr2O3-H2SO4 2: NaOBr View Scheme
参考文献
Journal of the American Chemical Society, , vol. 55, p. 4209,4212
参考文献
Journal of the American Chemical Society, , vol. 61, p. 965
反应条件
potassium permanganate
参考文献
Journal of the American Chemical Society, , vol. 74, p. 4073,4075
反应条件
hydrogenchloride in acetonitrile 24 h; Heating;
参考文献
Stang, Peter J.; Roberts, Kenneth A.
Journal of Organic Chemistry, 1987 , vol. 52, # 23 p. 5213 - 5217
反应条件
1: alcoholic KOH 2: water / 275 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 71, p. 698,700
反应条件
water; difluoro[4-(trifluoromethyl)phenyl]-λ(3)-bromane in dichloromethane T=0°C; Baeyer-Villiger type oxidation; 1 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 132, # 27 p. 9236 - 9239
反应条件
copper(II) oxide T=300°C; Gas phase;
参考文献
The NutraSweet Company
Patent: EP1186591 A2, 2002 ;
Location in patent: Page column 3 ;
反应条件
KHF2; dihydrogen peroxide in acetic anhydride; N,N-dimethyl-formamide 20 h; Ambient temperature; Yield given;
参考文献
Tetrahedron Letters, , vol. 25, # 3 p. 321 - 324
反应条件
1: N2H4 / triethylene glycol 2: KOH / Heating View Scheme
参考文献
Chimia, , vol. 57, # 11 p. 697 - 701