4-(2,2,2-三氟-1-羟基乙基)苯甲腈合成路线 （共 5 条）
反应条件
1: With potassium carbonate in N,N-dimethyl-formamide T=20°C; 4 h; 2: With water in N,N-dimethyl-formamide 4 h; Acidic conditions;
参考文献
Cheng, Huicheng; Pei, Yu; Leng, Faqiang; Li, Jingya; Liang, Apeng; Zou, Dapeng; Wu, Yangjie; Wu, Yusheng
Tetrahedron Letters, 2013 , vol. 54, # 33 p. 4483 - 4486
反应条件
tetrakis(dimethylamino)ethylene in N,N-dimethyl-formamide T=-20 - 20°C; 8.16667 h; Irradiation;
参考文献
Ait-Mohand, Samia; Takechi, Naoto; Medebielle, Maurice; Dolbier Jr., William R.
Organic Letters, 2001 , vol. 3, # 26 p. 4271 - 4273
反应条件
zinc in pyridine T=40°C; P=1500.1 - 3000.2 Torr; 4 h;
参考文献
Tordeux, Marc; Francese, Catherine; Wakselman, Claude
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 7 p. 1951 - 1957
反应条件
1: 1,3-bis(1-adamantyl)-2-imidazolidene / dimethylformamide / -25 - 20 °C 2: 0.98 g / HCl / dimethylformamide; H2O / 20 °C View Scheme
参考文献
Song, Jinhua J.; Tan, Zhulin; Reeves, Jonathan T.; Gallou, Fabrice; Yee, Nathan K.; Senanayake, Chris H.
Organic Letters, 2005 , vol. 7, # 11 p. 2193 - 2196
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in ethyl acetate 19 h; Reflux;
参考文献
Cheng, Huicheng; Pei, Yu; Leng, Faqiang; Li, Jingya; Liang, Apeng; Zou, Dapeng; Wu, Yangjie; Wu, Yusheng
Tetrahedron Letters, 2013 , vol. 54, # 33 p. 4483 - 4486
