3-氯-4-乙基苯并[E][1,2,4]噻二嗪1,1-二氧化物合成路线 （共 5 条）
参考文献
Taiho Pharmaceutical Co. Ltd.
Patent: US5401739 A1, 1995 ;
反应条件
1: nitromethane / 0.5 h / 0 - 20 °C 2: aluminium chloride / 0.5 h / 120 °C 3: PCl5 / 0.5 h / 190 °C View Scheme
参考文献
Reddy; Kamal; Bhaskar Rao; Sattur
European Journal of Medicinal Chemistry, 1986 , vol. 21, # 2 p. 177 - 179
反应条件
1: 86 percent / hydrazine hydrate (98percent) / CHCl3 / 0.5 h / Ambient temperature 2: 65 percent / hydrochloric acid / methanol / 3 h / Heating View Scheme
参考文献
Reddy, A. V. N.; Kamal, Ahmed; Sattur, P. B.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 1295 - 1297
反应条件
1: 86 percent / hydrazine hydrate (98percent) / CHCl3 / 0.5 h / Ambient temperature 2: 53 percent / hydrochloric acid / ethanol / 4 h / Heating View Scheme
参考文献
Reddy, A. V. N.; Kamal, Ahmed; Sattur, P. B.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 1295 - 1297
反应条件
hydrazine hydrate in chloroform 0.5 h; Ambient temperature;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 24, p. 1295 - 1297
