tetrabutyl ammonium fluoride in tetrahydrofuran
T=70°C; 12 h; Inert atmosphere;
参考文献
Krishnan, Shyam; Bagdanoff, Jeffrey T.; Ebner, David C.; Ramtohul, Yeeman K.; Tambar, Uttam K.; Stoltz, Brian M.
Journal of the American Chemical Society, 2008 , vol. 130, # 41 p. 13745 - 13754
With potassium carbonate; thiophenol in N,N-dimethyl-formamide T=23°C; 12 h; Inert atmosphere;
参考文献
Krishnan, Shyam; Bagdanoff, Jeffrey T.; Ebner, David C.; Ramtohul, Yeeman K.; Tambar, Uttam K.; Stoltz, Brian M. Journal of the American Chemical Society, 2008 , vol. 130, # 41 p. 13745 - 13754
Stage #1: With hydrogenchloride in 1,4-dioxane; methanol T=20°C; 0.583333 h; Inert atmosphere; Stage #2: With sodium hydrogencarbonate in 1,4-dioxane; methanol; water Inert atmosphere;
参考文献
Brak, Katrien; Ellman, Jonathan A. Organic Letters, 2010 , vol. 12, # 9 p. 2004 - 2007
