反应条件
hydrogenchloride; magnesium in tetrahydrofuran byproducts: C6H4(OMe)2; N2-atmosphere; dropwise addn. of aryl bromide to Mg, heating to 60°C for 3 h, addn. of borate at -78°C, warming to room temp., addn. of 4 M HCl; extn. into Et2O, drying (MgSO4), solvent removal (reduced pressure), sublimation off of C6H4(OMe)2 (vac.), recrystn. (hexanes);
参考文献
Hyslop, Alison G.; Therien, Michael J.
Inorganica Chimica Acta, 1998 , vol. 275-276, p. 427 - 434
