6-氯-6-氧代己酸乙酯合成路线 （共 76 条）
反应条件
1: nitrobenzene; AlCl3
2: platinum; acetic acid / Hydrogenation
View Scheme
参考文献
Duschinsky; Dolan
Journal of the American Chemical Society, 1945 , vol. 67, p. 2079,2082
反应条件
1: 1) AlCl3 / 1) nitrobenzene, 10 deg C, 0.5h, 2) 65 deg C, 4h
2: 62 percent / NaBH4 / methanol / 2.5 h / Ambient temperature
3: 1) piperidine, 2) glacial HOAc / 1) MeOH, 8h, reflux, 2) 60 deg C, 10h
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参考文献
Baxter, Robert L.; Camp, Dominic J.; Coutts, Andrew; Shaw, Nicholas
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 2 p. 255 - 258
反应条件
aluminium trichloride; nitrobenzene
参考文献
Duschinsky; Dolan
Journal of the American Chemical Society, 1945 , vol. 67, p. 2079,2082
反应条件
1: zinc chloride / 0 °C
2: alcohol. KOH-solution / anschliessendes Hydrieren an Palladium/Calciumcarbonat
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参考文献
Crombie; Griffin
Journal of the Chemical Society, 1958 , p. 4435,4443
反应条件
1: K2CO3; aqueous dioxane
2: platinum; methanol / Hydrogenation
3: ethanol. KOH-solution
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参考文献
Zahn; Lauer
Makromolekulare Chemie, 1957 , vol. 23, p. 85,116
反应条件
1: nitrobenzene; AlCl3 / Beim Erwaermen des Reaktionsprodukts in wss. NaOH
2: platinum; acetic acid / Hydrogenation
View Scheme
参考文献
Duschinsky; Dolan
Journal of the American Chemical Society, 1946 , vol. 68, p. 2350,2353
