反应条件
1: 1.) borane, 2-methyl-2-butene, 2.) 30percent aq. H2O2 / 1.) THF, 0 deg C, 1 h, 2.) THF, H2O, 0 deg C, 30 min
2: Et3N / CH2Cl2 / 24 h / 0 °C
3: tetrahydrofuran / 48 h / 80 °C
View Scheme
参考文献
Theodore; Nelson
Journal of Organic Chemistry, 1987 , vol. 52, # 7 p. 1309 - 1315
