反应条件
1: 82 percent / H2 / 10percent Pd/C, 70percent HClO4 / methanol / 25 °C / 2068.6 Torr
2: 2.) DIBAL / 1. 90 gradC, 50 h; 2. THF, 0 gradC, 1 h.
View Scheme
参考文献
Wender, Paul A.; Fisher, Karl
Tetrahedron Letters, 1986 , vol. 27, # 17 p. 1857 - 1860
