4-甲基-1,3-二氧戊环合成路线 （共 7 条）
参考文献
Burczyk, Bogdan
Journal fuer Praktische Chemie (Leipzig), 1980 , vol. 322, # 1 p. 173 - 176
反应条件
zinc(II) chloride T=130 - 150°C;
参考文献
Brusilovskii, Yu. E.; Kuznetsov
Russian Journal of General Chemistry, 2011 , vol. 81, # 3 p. 542 - 544
反应条件
zinc(II) chloride T=130 - 150°C;
参考文献
Brusilovskii, Yu. E.; Kuznetsov
Russian Journal of General Chemistry, 2011 , vol. 81, # 3 p. 542 - 544
反应条件
phosphoric acid T=100°C; im Rohr;
参考文献
Journal of the Chemical Society, , vol. 101, p. 1804
反应条件
sulfuric acid; water
参考文献
US2182754 , ;
DE664272 , ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 25, p. 55
反应条件
lithium aluminium tetrahydride; boron trichloride 1.) CH2Cl2, 10 min, 2.) Et2O, 30 min; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bonner, Trevor G.; Lewis, David; Rutter, Keith
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1807 - 1810
反应条件
lithium aluminium tetrahydride; boron trichloride 1.) CH2Cl2, 10 min, 2.) Et2O, 30 min; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bonner, Trevor G.; Lewis, David; Rutter, Keith
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1807 - 1810
