N-BOC-L-环己基甘氨酸合成路线 （共 8 条）
反应条件
1: NEt3 / tetrahydrofuran / -10 °C 2: 66 percent / NaBH4 / H2O / 0 °C View Scheme
参考文献
Bioorganic and medicinal chemistry letters, , vol. 14, # 1 p. 275 - 278
反应条件
sodium tetrahydroborate; calcium chloride in tetrahydrofuran; ethanol T=-5°C; 5 h;
参考文献
Journal of Organic Chemistry, , vol. 52, # 8 p. 1487 - 1492
反应条件
1: n-BuLi / tetrahydrofuran / -78 - 20 °C 2: 6percent Na-Hg, Na2HPO4 / methanol / 3 h / 0 - 20 °C 3: PPTS / ethanol / 6 h / 50 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 35, # 2 p. 237 - 240
反应条件
1: aq. NaOH / dioxane / 20 °C 2: NEt3 / tetrahydrofuran / -10 °C 3: 66 percent / NaBH4 / H2O / 0 °C View Scheme
参考文献
Bioorganic and medicinal chemistry letters, , vol. 14, # 1 p. 275 - 278
反应条件
1: aq. NaOH / dioxane / 20 °C 2: NEt3 / tetrahydrofuran / -10 °C 3: 66 percent / NaBH4 / H2O / 0 °C View Scheme
参考文献
Bioorganic and medicinal chemistry letters, , vol. 14, # 1 p. 275 - 278
反应条件
1: n-BuLi / tetrahydrofuran / -78 - 20 °C 2: 6percent Na-Hg, Na2HPO4 / methanol / 3 h / 0 - 20 °C 3: PPTS / ethanol / 6 h / 50 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 35, # 2 p. 237 - 240
反应条件
1: 6percent Na-Hg, Na2HPO4 / methanol / 3 h / 0 - 20 °C 2: PPTS / ethanol / 6 h / 50 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 35, # 2 p. 237 - 240
反应条件
chromium(VI) oxide; sulfuric acid T=0 - 20°C; 1 h; Yield given;
参考文献
Tetrahedron Letters, , vol. 35, # 2 p. 237 - 240
