3-(苯甲酰基氧基)-5-溴-2-羟基苯甲酸合成路线 （共 4 条）
反应条件
bromine; sodium acetate in acetic acid T=70°C; 3 h;
参考文献
Hogberg; De Paulis; Johansson; Kumar; Hall; Ogren
Journal of Medicinal Chemistry, 1990 , vol. 33, # 8 p. 2305 - 2309
反应条件
1: 61 percent / K2CO3 / dimethylformamide / 8 h / 80 °C 2: 80 percent / bromine, sodium acetate / acetic acid / 3 h / 70 °C View Scheme
参考文献
Hogberg; De Paulis; Johansson; Kumar; Hall; Ogren
Journal of Medicinal Chemistry, 1990 , vol. 33, # 8 p. 2305 - 2309
反应条件
1: 61 percent / K2CO3 / dimethylformamide / 8 h / 80 °C 2: 80 percent / bromine, sodium acetate / acetic acid / 3 h / 70 °C View Scheme
参考文献
Hogberg; De Paulis; Johansson; Kumar; Hall; Ogren
Journal of Medicinal Chemistry, 1990 , vol. 33, # 8 p. 2305 - 2309
反应条件
sodium hydride 1.) DMSO, RT, 2 h, 2.) 60 deg C, 2 h; Multistep reaction;
参考文献
Hogberg; De Paulis; Johansson; Kumar; Hall; Ogren
Journal of Medicinal Chemistry, 1990 , vol. 33, # 8 p. 2305 - 2309
