(3aS,7aS)-1,3-二[(4-溴苯基)甲基]-2-(2E)-2-丁烯-1-基-2-氯八氢-1H-1,3,2-苯并二氮杂硅杂环戊烯合成路线 （共 3 条）
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane T=20°C; 12 h; Cooling;
参考文献
Vuong, Sophie; Brondel, Nicolas; Len, Christophe; Papot, Sebastien; Renoux, Brigitte
Tetrahedron, 2012 , vol. 68, # 2 p. 433 - 439
反应条件
1: sodium tetrahydroborate / methanol / 0 °C / Inert atmosphere; Reflux 2: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 12 h / 20 °C / Cooling View Scheme
参考文献
Vuong, Sophie; Brondel, Nicolas; Len, Christophe; Papot, Sebastien; Renoux, Brigitte
Tetrahedron, 2012 , vol. 68, # 2 p. 433 - 439
反应条件
1: methanesulfonic acid; potassium carbonate / ethanol; dichloromethane; water / 13 h / 20 °C / Inert atmosphere; Reflux 2: sodium tetrahydroborate / methanol / 0 °C / Inert atmosphere; Reflux 3: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 12 h / 20 °C / Cooling View Scheme
参考文献
Vuong, Sophie; Brondel, Nicolas; Len, Christophe; Papot, Sebastien; Renoux, Brigitte
Tetrahedron, 2012 , vol. 68, # 2 p. 433 - 439
