5-碘-1-甲基-1H-吲唑合成路线 （共 3 条）
反应条件
1: With sulfuric acid; sodium nitrite in water T=0°C; 0.166667 h; 2: With sodium iodide in water T=0 - 90°C; 0.333333 h; 3: With sodium hydroxide; water
参考文献
VERTEX PHARMACEUTICALS INCORPORATED
Patent: WO2008/128009 A2, 2008 ;
Location in patent: Page/Page column 47-48 ;
WO 2008/128009 A2
反应条件
tert.-butylnitrite in tetrahydrofuran 1 h; Reflux;
参考文献
Liu, Han-Jun; Hung, Shiang-Fu; Chen, Chuan-Lin; Lin, Mei-Huey
Tetrahedron, 2013 , vol. 69, # 19 p. 3907 - 3912
反应条件
1: ethanol / |Reflux 2: tert.-butylnitrite / tetrahydrofuran / 1 h / |Reflux View Scheme
参考文献
Tetrahedron, , vol. 69, # 19 p. 3907 - 3912
