1-氟-2,4,6-三甲基吡啶三氟甲烷磺酸盐合成路线 (共 7 条)
反应条件
argon; fluorine in acetonitrile T=-40°C;
参考文献
Tetrahedron, , vol. 49, # 11 p. 2151 - 2158
反应条件
fluorine in acetonitrile T=-40°C;
参考文献
Tetrahedron Letters, , vol. 27, # 28 p. 3271 - 3274
反应条件
fluorine; NAF in acetonitrile T=-40°C; 3 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 64, # 4 p. 1081 - 1092
反应条件
fluorine in water; acetonitrile T=-40°C; 3 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 64, # 4 p. 1081 - 1092
参考文献
Bulletin of the Chemical Society of Japan, , vol. 64, # 4 p. 1081 - 1092
反应条件
N-bromosuccinmide
1.) CH2Cl2, r.t., 4 h; 2.) CH2Cl2, MeOH, H2O, r.t., 0.5 h; Yield given. Multistep reaction;
参考文献
Umemoto, Teruo; Tomizawa, Ginjiro
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, # 11 p. 3625 - 3630
反应条件
in dichloromethane
4 h; Ambient temperaturefurther triflate; Mechanism;
参考文献
Umemoto, Teruo; Tomizawa, Ginjiro
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, # 11 p. 3625 - 3630