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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
107292-13-7
合成路线
(共 7 条)
107292-13-7
+
103-67-3
N-甲基苄胺
→
反应条件
107292-20-6
+
86799-77-1
3,6-二(1-甲基乙基)-2(1H)-吡嗪酮
反应条件
triethylamine in acetonitrile 0.166667 h; Ambient temperature;
参考文献
Ohta, Akihiro; Inagawa, Yukiko; Mitsugi, Chie
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 1643 - 1646
107292-13-7
+
100-46-9
苄胺
→
反应条件
102276-50-6
+
86799-77-1
3,6-二(1-甲基乙基)-2(1H)-吡嗪酮
反应条件
triethylamine in acetonitrile 0.166667 h; Ambient temperature;
参考文献
Ohta, Akihiro; Inagawa, Yukiko; Mitsugi, Chie
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 1643 - 1646
107292-13-7
→
反应条件
107292-11-5
反应条件
Multi-step reaction with 2 steps 1: Triethylamine / acetonitrile / 0.17 h / Ambient temperature2: 1)NaH 3)pyridine / 1)dioxane, room temp. 2)overnight, room temp. 3)overnight, room temp.
参考文献
Ohta, Akihiro; Inagawa, Yukiko; Mitsugi, Chie Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 1643 - 1646
107292-13-7
→
反应条件
107292-12-6
反应条件
Multi-step reaction with 2 steps 1: Triethylamine / acetonitrile / 0.17 h / Ambient temperature2: 1)NaH 3)pyridine / 1)dioxane, room temp. 2)overnight, room temp. 3)overnight, room temp.
参考文献
Ohta, Akihiro; Inagawa, Yukiko; Mitsugi, Chie Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 1643 - 1646
107292-11-5
→
反应条件
107292-13-7
反应条件
Multi-step reaction with 2 steps 1: Triethylamine / H2O; acetonitrile / 24 h / Ambient temperature2: 1)NaH 3)pyridine / 1)dioxane, room temp. 2)overnight, room temp. 3)overnight, room temp.
参考文献
Ohta, Akihiro; Inagawa, Yukiko; Mitsugi, Chie Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 1643 - 1646
107292-12-6
→
反应条件
107292-13-7
反应条件
Multi-step reaction with 2 steps 1: Triethylamine / H2O; acetonitrile / 24 h / Ambient temperature2: 1)NaH 3)pyridine / 1)dioxane, room temp. 2)overnight, room temp. 3)overnight, room temp.
参考文献
Ohta, Akihiro; Inagawa, Yukiko; Mitsugi, Chie Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 1643 - 1646
107292-10-4
→
反应条件
107292-13-7
反应条件
Multi-step reaction with 2 steps 1: Triethylamine / acetonitrile / 0.17 h / Ambient temperature2: 1)NaH 3)pyridine / 1)dioxane, room temp. 2)overnight, room temp. 3)overnight, room temp.
参考文献
Ohta, Akihiro; Inagawa, Yukiko; Mitsugi, Chie Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 1643 - 1646