4-(羟甲基)苯硼酸甲基亚氨基二乙酸酯合成路线 (共 7 条)
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane DDQ, CH2Cl2, 23°C, 1.5 h;
参考文献
Gillis, Eric P.; Burke, Martin D.
Journal of the American Chemical Society, 2008 , vol. 130, # 43 p. 14084 - 14085
反应条件
pyridine hydrogenfluoride in tetrahydrofuran T=23°C; 0.333333 h; Inert atmosphere;
参考文献
Gillis, Eric P.; Burke, Martin D.
Journal of the American Chemical Society, 2008 , vol. 130, # 43 p. 14084 - 14085
反应条件
sodium tetrahydroborate in tetrahydrofuran; ethanol T=0°C; Inert atmosphere;
参考文献
Gillis, Eric P.; Burke, Martin D.
Journal of the American Chemical Society, 2008 , vol. 130, # 43 p. 14084 - 14085
反应条件
in dimethyl sulfoxide; toluene 3 h; RefluxInert atmosphere;
参考文献
Gillis, Eric P.; Burke, Martin D.
Journal of the American Chemical Society, 2008 , vol. 130, # 43 p. 14084 - 14085
反应条件
in tetrahydrofuran HF*pyridine, THF, 23°C, 20 min;
参考文献
Gillis, Eric P.; Burke, Martin D.
Journal of the American Chemical Society, 2008 , vol. 130, # 43 p. 14084 - 14085
反应条件
in tetrahydrofuran; ethanol NaBH4, ethanol:THF, 0°C, 2 h;
参考文献
Gillis, Eric P.; Burke, Martin D.
Journal of the American Chemical Society, 2008 , vol. 130, # 43 p. 14084 - 14085
反应条件
sodium hydroxide; water in tetrahydrofuran T=23°C; 0.166667 h; Inert atmosphere;
参考文献
Gillis, Eric P.; Burke, Martin D.
Journal of the American Chemical Society, 2008 , vol. 130, # 43 p. 14084 - 14085