反应条件
1: 2-bromo-4-flouro-1-iodobenzene With isopropylmagnesium chloride in tetrahydrofuran T=-30 - -25°C; 0.5 h; Inert atmosphereLarge scale; 2: 1,1,1-trifluoro-4-methyl-pent-3-en-2-one With copper(l) iodide in tetrahydrofuran T=-30 - -25°C; 4 h; Inert atmosphereLarge scale;
参考文献
Journal of Organic Chemistry, , vol. 78, # 8 p. 3616 - 3635