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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-氯苯乙烯
合成路线
（共 400 条）
1073-67-2
4-氯苯乙烯
+
111966-93-9
→
反应条件
2510-74-9
+
1256837-53-2
反应条件
(SPY-5-31)-dichloro-(κ2(C,O)-(2-isopropyloxybenzylidene))(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)ruthenium in dichloromethane T=25°C; 1 h; Inert atmosphereMolecular sieve; stereoselective reaction;
参考文献
Junker, Christopher S.; Welker, Mark E.; Day, Cynthia S.
Journal of Organic Chemistry, 2010 , vol. 75, # 23 p. 8155 - 8165
292638-84-7
+
1073-67-2
4-氯苯乙烯
→
反应条件
103-30-0
反式-1,2-二苯乙烯
+
2510-74-9
+
1657-50-7
反应条件
RuCl2(=CHPh)[1,3-ImH2]P(Cy)3 in dichloromethane T=40°C; 2 h;
参考文献
Chang, Sukbok; Na, Youngim; Shin, Hyun Jung; Choi, Eunjung; Jeong, Lak Shin
Tetrahedron Letters, 2002 , vol. 43, # 41 p. 7445 - 7448
1073-67-2
4-氯苯乙烯
+
2628-16-2
→
反应条件
2510-74-9
+
47241-75-8
反应条件
RuCl2(=CHPh)[1,3-ImH2]P(Cy)3 in dichloromethane T=40°C; 2 h;
参考文献
Chang, Sukbok; Na, Youngim; Shin, Hyun Jung; Choi, Eunjung; Jeong, Lak Shin
Tetrahedron Letters, 2002 , vol. 43, # 41 p. 7445 - 7448
1073-67-2
4-氯苯乙烯
+
106-39-8
→
反应条件
2510-74-9
+
2642-81-1
反应条件
N,N-dicyclohexylmethylamine; tetrabutylammomium bromide; [ClPd(3-OH-5-CH(Me)=N(OH)-phenyl)]2 in N,N-dimethyl acetamide; water T=120°C; Heck reaction; 15 h; Product distribution; Further Variations:Reagentsreaction times;
参考文献
Alacid, Emilio; Najera, Carmen
Synlett, 2006 , # 18 p. 2959 - 2964
1073-67-2
4-氯苯乙烯
+
637-87-6
→
反应条件
2510-74-9
+
2642-81-1
反应条件
N,N-dicyclohexylmethylamine; tetrabutylammomium bromide; [ClPd(3-OH-5-CH(Me)=N(OH)-phenyl)]2 in N,N-dimethyl acetamide; water T=120°C; Heck reaction; 9 h; Product distribution; Further Variations:SolventsReagentsreaction times;
参考文献
Alacid, Emilio; Najera, Carmen
Synlett, 2006 , # 18 p. 2959 - 2964
1073-67-2
4-氯苯乙烯
+
637-87-6
→
反应条件
2510-74-9
反应条件
polymeric di(2-pyridyl)methylamine-based PdCl2; tetrabutylammomium bromide; diisopropylamine in water T=100°C; Heck reaction; 48 h; Product distribution; Further Variations:ReagentsTemperaturesreaction time;
参考文献
Gil-Molto, Juan; Karlstroem, Sofia; Najera, Carmen
Tetrahedron, 2005 , vol. 61, # 51 p. 12168 - 12176
1073-67-2
4-氯苯乙烯
→
反应条件
152714-07-3
反应条件
1: 91 percent / Zn-Cu; POCl3 / diethyl ether / 20 h / 20 °C 2: 93 percent / Zn; AcOH / 14 h / 20 °C View Scheme
参考文献
Wiberg, Kenneth B.; Shobe, David; Nelson, Gordon L.
Journal of the American Chemical Society, 1993 , vol. 115, # 23 p. 10645 - 10652
1073-67-2
4-氯苯乙烯
+
76-02-8
→
反应条件
152714-07-3
反应条件
zinc; trichlorophosphate 1.) Et2O, reflux; 2.) AcOH, reflux; Yield given. Multistep reaction;
参考文献
Mazzini, Claudio; Lebreton, Jacques; Alphand, Veronique; Furstoss, Roland
Tetrahedron Letters, 1997 , vol. 38, # 7 p. 1195 - 1196
1073-67-2
4-氯苯乙烯
→
反应条件
138476-26-3
反应条件
1: With Grubb's 2nd generation catalyst in toluene T=80°C; 1.5 h; Inert atmosphere; 2: With Grubb's 2nd generation catalyst; tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide in water; toluene; acetonitrile T=20°C; 1 h; Inert atmosphere;
参考文献
Schmidt, Bernd; Krehl, Stefan; Hauke, Sylvia
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5427 - 5435
1073-67-2
4-氯苯乙烯
→
反应条件
16396-62-6
反应条件
1: With magnesium in tetrahydrofuran T=60°C; 2 h; 2: With tributoxyborane in tetrahydrofuran T=-78 - 20°C; Further stages.;
参考文献
Qin, Yang; Sukul, Vishad; Pagakos, Dimitrios; Cui, Chengzhong; Jaekle, Frieder
Macromolecules, 2005 , vol. 38, # 22 p. 8987 - 8990
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