4-甲基-3-戊烯基硼酸频那醇酯合成路线 （共 3 条）
反应条件
1: 5-Bromo-2-methyl-pent-2-ene With magnesium in tetrahydrofuran 4 h; Inert atmosphereReflux; 2: 2-isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane in tetrahydrofuran T=-78 - 20°C; Inert atmosphere;
参考文献
Aggarwal, Varinder K.; Ball, Liam T.; Carobene, Simon; Connelly, Rickki L.; Hesse, Matthew J.; Partridge, Benjamin M.; Roth, Philippe; Thomas, Stephen P.; Webster, Matthew P.
Chemical Communications, 2012 , vol. 48, # 74 p. 9230 - 9232
反应条件
1: tetrahydrofuran / -78 - 20 °C / Inert atmosphere 2: hydrogenchloride; water / tetrahydrofuran / 0 - 20 °C / Inert atmosphere 3: diethyl ether; pentane / 48 h / Inert atmosphere View Scheme
参考文献
Elford, Tim G.; Nave, Stefan; Sonawane, Ravindra P.; Aggarwal, Varinder K.
Journal of the American Chemical Society, 2011 , vol. 133, # 42 p. 16798 - 16801
反应条件
in diethyl ether; pentane 48 h; Inert atmosphere;
参考文献
Elford, Tim G.; Nave, Stefan; Sonawane, Ravindra P.; Aggarwal, Varinder K.
Journal of the American Chemical Society, 2011 , vol. 133, # 42 p. 16798 - 16801
