2-氨基-5-氯苯硼酸频那醇酯合成路线 （共 3 条）
反应条件
palladium diacetate; triethylamine; 2-dicyclohexylphosphino-1,1'-biphenyl in 1,4-dioxane T=80°C; Suzuki coupling; 1 h; Inert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 51, # 24 p. 5920 - 5923
反应条件
1: tetrahydrofuran / 1 h / 20 °C / |Inert atmosphere; |Glovebox 2: bis(η4-1,5-cyclooctadiene)-di-μ-methoxy-diiridium(I); 3,4,7,8-tetra-methyl-1,10-phenanthroline / tetrahydrofuran / 16 h / 80 °C / |Inert atmosphere; |Glovebox 3: methanol / tetrahydrofuran / 20 °C / |Inert atmosphere; |Glovebox View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 49 p. 12915 - 12919
Angew. Chem., , vol. 125, # 49 p. 13153 - 13157,5
反应条件
1: bis(η4-1,5-cyclooctadiene)-di-μ-methoxy-diiridium(I); 3,4,7,8-tetra-methyl-1,10-phenanthroline / tetrahydrofuran / 16 h / 80 °C / |Inert atmosphere; |Glovebox 2: methanol / tetrahydrofuran / 20 °C / |Inert atmosphere; |Glovebox View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 49 p. 12915 - 12919
Angew. Chem., , vol. 125, # 49 p. 13153 - 13157,5
