2-氨基-3-溴-5-苯基吡啶合成路线 （共 8 条）
反应条件
formic acid; 5 platinum on carbon; triethylamine in acetonitrile Cooling with iceReflux;
参考文献
Filace, Fabiana; Sucunza, David; Izquierdo, M. Luisa; Burgos, Carolina; Alvarez-Builla, Julio
Tetrahedron, 2013 , vol. 69, # 30 p. 6088 - 6094
反应条件
bromine in acetic acid T=0 - 20°C;
参考文献
Chrisman; Knize; Tanga
Journal of Heterocyclic Chemistry, 2008 , vol. 45, # 6 p. 1641 - 1649
反应条件
1: 58 percent / NaNH2 / toluene 2: 3.1 g / Br2 / acetic acid / 1 h / Ambient temperature View Scheme
参考文献
Heterocycles, , vol. 24, # 7 p. 1815 - 1819
反应条件
1: N-bromosuccinmide / dichloromethane / 3 h / 20 °C 2: formic acid; triethylamine; 5 platinum on carbon / acetonitrile / |Cooling with ice; |Reflux View Scheme
参考文献
Tetrahedron, , vol. 69, # 30 p. 6088 - 6094
反应条件
1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / ethanol; toluene / 12 h / |Inert atmosphere; |Reflux 2: N-bromosuccinmide / dichloromethane / 3 h / 20 °C 3: formic acid; triethylamine; 5 platinum on carbon / acetonitrile / |Cooling with ice; |Reflux View Scheme
参考文献
Tetrahedron, , vol. 69, # 30 p. 6088 - 6094
反应条件
1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / ethanol; toluene / 12 h / |Inert atmosphere; |Reflux 2: N-bromosuccinmide / dichloromethane / 3 h / 20 °C 3: formic acid; triethylamine; 5 platinum on carbon / acetonitrile / |Cooling with ice; |Reflux View Scheme
参考文献
Tetrahedron, , vol. 69, # 30 p. 6088 - 6094
反应条件
copper(II) sulfate in water T=200°C; 72 h; Heating;
参考文献
Heterocycles, , vol. 24, # 7 p. 1815 - 1819
反应条件
1: CuSO4 / H2O / 72 h / 200 °C / Heating 2: ethanol / 1 h / 175 °C View Scheme
参考文献
Knize, Mark G.; Felton, James S.
Heterocycles, 1986 , vol. 24, # 7 p. 1815 - 1819
