1: 1.) NaOH, 2.) HCl / 1.) H2O, MeOH, -30 deg C to r.t., 2.) r.t.
2: 92 percent / POCl3 / 18 h / 170 - 175 °C
View Scheme
参考文献
Sato, Nobuhiro; Matsumoto, Kaori; Takishima, Masayuki; Mochizuki, Katsura
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 21 p. 3167 - 3172
Shibanov, V. V.; Mizyuk, V. L.; Milyashkevich, P. E.
Journal of Organic Chemistry USSR (English Translation), 1982 , p. 964 - 965
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 5 p. 1113 - 1114
Kroutil, Wolfgang; Lasterra-Sanchez, M. Elena; Maddrell, Samuel J.; Mayon, Patrick; Morgan, Phillip; Roberts, Stanley M.; Thornton, Steven R.; Todd, Christine J.; Tueter, Melek
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 23 p. 2837 - 2844