in neat (no solvent) byproducts: benzene, chlorobenzene; passing through tubular quartz reactor (contact time 30 s, temperature 500°C; yield 9.8 and 11.3percent at 550°C depending on the reactant ratio); products condensing;
参考文献
Chernyshev; Komalenkova; Yakovleva; Bykovchenko; Khromykh; Bochkarev; Shcherbinin
Russian Journal of General Chemistry, 1999 , vol. 69, # 9 p. 1406 - 1409
in neat (no solvent)
byproducts: N2, ClCH2CO2CH2CH3; 1 equiv of diazoester adding slowly to an equimolar mixt. of Ge and Sn deriv. to result in exothermic reaction with N2 evolution; after 4 h at 20°C concg., diene ligand adding, heating in a sealed tube for 12h at 120°C; analyzed by gas chromy. and NMR spectroscopy;
参考文献
Castel, A.; Riviere, P.; Satge, J.
Journal of Organometallic Chemistry, 1982 , vol. 232, # 2 p. 137 - 146
